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105648 HPTLC Silica gel 60 F₂₅₄ Premium Purity

105648
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Overview

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Key Specifications Table

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      Fibre case 50 units
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      Description
      Catalogue Number105648
      OverviewIdeal for advanced pharmacopoeia applications, this high-performance plate keeps separations free of contamination. The plate is highly pure and exhibits minimal background, even with middle-polar solvent systems. Its separation performance is an exact match to the related HPTLC plate product. Based on the proven HPTLC 60 F254 plate, the HPTLC premium purity plate comes carefully wrapped in a special, plastic-coated aluminum foil. This prevents plasticizers (such as phthalates) from leaving deposits. Without the foil, the plasticizers could appear as an “unknown extra zone” when mid-polar solvent systems (such as toluene/ethyl acetate (95/5)) are in use, and they could be stained by derivatization reagents (such as anis aldehyde).
      References
      Product Information
      HS Code3822 00 00
      Quality LevelMQ100
      Applications
      ApplicationGlass HPTLC Silica gel 60 F₂₅₄ Premium Purity plates. Silica gel HPTLC plates size 20 x 10 cm, 50 sheets.
      Biological Information
      Physicochemical Information
      Dimensions
      Materials Information
      Toxicological Information
      Safety Information according to GHS
      Storage class10 - 13 Other liquids and solids
      Safety Information
      Product Usage Statements
      Storage and Shipping Information
      StorageStore at +2°C to +30°C.
      Packaging Information
      Transport Information
      Supplemental Information
      Specifications
      Specific surface area (according to BET; 5-Pt. measurement)480 - 540 m²/g
      Pore volume (N₂-isotherm)0.74 - 0.84 ml/g
      d 50 (laser diffraction, size distribution)5 - 7 µm
      Layer thickness150 - 200 µm
      Deviation of layer thickness per plate≤ 35 µm
      Chromatographic testings:
      A) Colour test
      hRf-values
      - bleu vif organol, colour test, lipophile

      17 - 22
      - Ceres Black G, colour test, lipophile38 - 43
      - ceres Violet brn, colour test, lipophile58 - 64
      separation number
      - colourtest, lipophile

      ≥ 10.0
      B) Steroid test
      hRf-values
      - hydrocortisone, steroid test

      23 - 29
      - Reichstein S, steroid test36 - 45
      - methyltestosterone, steroid test43 - 52
      separation number
      - steroid test

      ≥ 10.5
      Typical value determined on a conditioned plate
      Eluent A) Toluene (45% rel.humidity)
      Eluent B) Ethyl acetate/Toluene (95+5 v/v; 20% rel.humidity)

      Documentation

      HPTLC Silica gel 60 F₂₅₄ Premium Purity SDS

      Title

      Safety Data Sheet (SDS) 

      HPTLC Silica gel 60 F₂₅₄ Premium Purity Certificates of Analysis

      Product Number PackagingSpecificationLot Number
      1056480001 Fibre casePDF Specification Document

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      Categories

      Analytics and Sample Preparation > Analytical Chromatography > Thin-Layer Chromatography (TLC) Products > High Performance Thin-Layer Chromatography Plates (HPTLC) > HPTLC Premium Purity Plate